Information card for entry 7002629

Structure parameters

• Formula: C62 H60 B2 Cl6 Cu F8 N2 O4 P4
• Calculated formula: C62 H60 B2 Cl6 Cu F8 N2 O4 P4
• Title of publication: Synthesis and reactivity of diphosphine metal complexes bearing peripheral ketenimine functionalities
• Authors of publication: Ruiz, Javier; Gonzalo, Marta P.; Vivanco, Marilín; Quesada, Roberto; Mosquera, Marta E. G.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 42
• Pages of publication: 9280
• a: 19.6068 ± 0.0002 Å
• b: 17.5173 ± 0.0002 Å
• c: 39.3124 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 13502.2 ± 0.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 9
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0692
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.1293
• Weighted residual factors for all reflections included in the refinement: 0.1405
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No