Information card for entry 7002630

Structure parameters

• Formula: C92 H93 B2 Cl4 Cu2 F8 N3 O2 P6
• Calculated formula: C92 H93 B2 Cl4 Cu2 F8 N3 O2 P6
• Title of publication: Synthesis and reactivity of diphosphine metal complexes bearing peripheral ketenimine functionalities
• Authors of publication: Ruiz, Javier; Gonzalo, Marta P.; Vivanco, Marilín; Quesada, Roberto; Mosquera, Marta E. G.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 42
• Pages of publication: 9280
• a: 14.212 ± 0.003 Å
• b: 40.569 ± 0.008 Å
• c: 17.545 ± 0.004 Å
• α: 90°
• β: 105.41 ± 0.03°
• γ: 90°
• Cell volume: 9752 ± 4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2364
• Residual factor for significantly intense reflections: 0.1684
• Weighted residual factors for significantly intense reflections: 0.4302
• Weighted residual factors for all reflections included in the refinement: 0.4585
• Goodness-of-fit parameter for all reflections included in the refinement: 1.47
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No