Crystallography Open Database

Information card for entry 7002965

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Coordinates	7002965.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H33 I6 P Sn
Calculated formula	C18 H33 I6 P Sn
Title of publication	The reaction of tin(iv) iodide with phosphines: formation of new halotin anions
Authors of publication	Apostolico, Leonardo; Kociok-Köhn, Gabriele; Molloy, Kieran C.; Blackman, Christopher S.; Carmalt, Claire J.; Parkin, Ivan P.
Journal of publication	Dalton Transactions
Year of publication	2009
Journal issue	47
Pages of publication	10486 - 10494
a	12.1215 ± 0.0001 Å
b	17.3964 ± 0.0001 Å
c	21.9965 ± 0.0002 Å
α	90°
β	103.533 ± 0.001°
γ	90°
Cell volume	4509.63 ± 0.06 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0845
Residual factor for significantly intense reflections	0.047
Weighted residual factors for significantly intense reflections	0.0935
Weighted residual factors for all reflections included in the refinement	0.1047
Goodness-of-fit parameter for all reflections included in the refinement	0.967
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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