Crystallography Open Database

Information card for entry 7002966

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Coordinates	7002966.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C72 H72 I12 P6 Sn3
Calculated formula	C72 H72 I12 P6 Sn3
Title of publication	The reaction of tin(iv) iodide with phosphines: formation of new halotin anions
Authors of publication	Apostolico, Leonardo; Kociok-Köhn, Gabriele; Molloy, Kieran C.; Blackman, Christopher S.; Carmalt, Claire J.; Parkin, Ivan P.
Journal of publication	Dalton Transactions
Year of publication	2009
Journal issue	47
Pages of publication	10486 - 10494
a	65.6481 ± 0.0005 Å
b	12.1063 ± 0.0001 Å
c	23.3971 ± 0.0002 Å
α	90°
β	104.324 ± 0.004°
γ	90°
Cell volume	18016.9 ± 0.4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1129
Residual factor for significantly intense reflections	0.0528
Weighted residual factors for significantly intense reflections	0.0907
Weighted residual factors for all reflections included in the refinement	0.1071
Goodness-of-fit parameter for all reflections included in the refinement	0.984
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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