Information card for entry 7003482

Structure parameters

• Formula: C8 H24 Li N Si2 Zn
• Calculated formula: C8 H23.397 Li N Si2 Zn
• Title of publication: Synthesis and structural elucidation of solvent-free and solvated lithium dimethyl (HMDS) zincates
• Authors of publication: Armstrong, David R.; Herd, Emma; Graham, David V.; Hevia, Eva; Kennedy, Alan R.; Clegg, William; Russo, Luca
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 10
• Pages of publication: 1323 - 1330
• a: 6.784 ± 0.0003 Å
• b: 13.9936 ± 0.0007 Å
• c: 15.8133 ± 0.0007 Å
• α: 90°
• β: 97.65 ± 0.002°
• γ: 90°
• Cell volume: 1487.84 ± 0.12 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1045
• Residual factor for significantly intense reflections: 0.0655
• Weighted residual factors for significantly intense reflections: 0.1251
• Weighted residual factors for all reflections included in the refinement: 0.1347
• Goodness-of-fit parameter for all reflections included in the refinement: 1.239
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No