Information card for entry 7003483

Structure parameters

• Formula: C17 H47 Li N4 Si2 Zn
• Calculated formula: C17 H47 Li N4 Si2 Zn
• SMILES: [Zn](C)(C)N([Si](C)(C)C)[Si](C)(C)C.[Li]12[N](CC[N]1(C)C)(C)CC[N]2(C)C
• Title of publication: Synthesis and structural elucidation of solvent-free and solvated lithium dimethyl (HMDS) zincates
• Authors of publication: Armstrong, David R.; Herd, Emma; Graham, David V.; Hevia, Eva; Kennedy, Alan R.; Clegg, William; Russo, Luca
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 10
• Pages of publication: 1323 - 1330
• a: 9.616 ± 0.003 Å
• b: 13.522 ± 0.004 Å
• c: 20.444 ± 0.006 Å
• α: 90°
• β: 100.676 ± 0.004°
• γ: 90°
• Cell volume: 2612.3 ± 1.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0281
• Residual factor for significantly intense reflections: 0.0227
• Weighted residual factors for significantly intense reflections: 0.0612
• Weighted residual factors for all reflections included in the refinement: 0.0642
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No