Information card for entry 7003524

Structure parameters

• Common name: (O(Li(thf)2(SiMeNCPhC(SiMe3)CPhN))2)
• Formula: C54 H76 Li2 N4 O5 Si4
• Calculated formula: C54 H76 Li2 N4 O5 Si4
• Title of publication: Synthesis and structures of some new types of lithium β-diketiminates
• Authors of publication: Wei, Xue-Hong; Farwell, James D.; Hitchcock, Peter B.; Lappert, Michael F.
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 8
• Pages of publication: 1073 - 1080
• a: 19.9377 ± 0.0001 Å
• b: 19.9377 ± 0.0001 Å
• c: 16.653 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6619.77 ± 0.09 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 6
• Space group number: 136
• Hermann-Mauguin space group symbol: P 42/m n m
• Hall space group symbol: -P 4n 2n
• Residual factor for all reflections: 0.0998
• Residual factor for significantly intense reflections: 0.0916
• Weighted residual factors for significantly intense reflections: 0.2847
• Weighted residual factors for all reflections included in the refinement: 0.2961
• Goodness-of-fit parameter for all reflections included in the refinement: 1.146
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No