Information card for entry 7003525

Structure parameters

• Common name: (O(SiMeNCPhCHCPhNLi(thf)2)2).(thf)
• Formula: C52 H68 Li2 N4 O6 Si2
• Calculated formula: C52 H68 Li2 N4 O6 Si2
• Title of publication: Synthesis and structures of some new types of lithium β-diketiminates
• Authors of publication: Wei, Xue-Hong; Farwell, James D.; Hitchcock, Peter B.; Lappert, Michael F.
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 8
• Pages of publication: 1073 - 1080
• a: 20.4546 ± 0.0005 Å
• b: 14.9128 ± 0.0004 Å
• c: 17.1049 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5217.6 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0849
• Residual factor for significantly intense reflections: 0.0605
• Weighted residual factors for significantly intense reflections: 0.1611
• Weighted residual factors for all reflections included in the refinement: 0.179
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No