Information card for entry 7003890

Structure parameters

• Common name: W(Cl)3(N(i-Pr)Ar)3
• Formula: C33.5 H49 Cl4 N3 W
• Calculated formula: C33.5 H49 Cl4 N3 W
• Title of publication: 6-Coordinate tungsten(vi) tris-n-isopropylanilide complexes: products of terminal oxo and nitrido transformations effected by main group electrophiles
• Authors of publication: Clough, Christopher R.; Müller, Peter; Cummins, Christopher C.
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 33
• Pages of publication: 4458 - 4463
• a: 10.7751 ± 0.0003 Å
• b: 13.3987 ± 0.0003 Å
• c: 13.5032 ± 0.0004 Å
• α: 88.852 ± 0.001°
• β: 71.987 ± 0.001°
• γ: 83.657 ± 0.001°
• Cell volume: 1842.38 ± 0.09 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0328
• Residual factor for significantly intense reflections: 0.0293
• Weighted residual factors for significantly intense reflections: 0.0826
• Weighted residual factors for all reflections included in the refinement: 0.0847
• Goodness-of-fit parameter for all reflections included in the refinement: 1.103
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No