Information card for entry 7003907

Structure parameters

• Formula: C36 H48 Fe Ge N2 O2
• Calculated formula: C36 H48 Fe Ge N2 O2
• Title of publication: Synthesis, characterisation and reactivity of germanium(ii) amidinate and guanidinate complexes
• Authors of publication: Jones, Cameron; Rose, Richard P.; Stasch, Andreas
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 21
• Pages of publication: 2871 - 2878
• a: 22.08 ± 0.004 Å
• b: 16.626 ± 0.005 Å
• c: 19.551 ± 0.005 Å
• α: 90°
• β: 109.6 ± 0.01°
• γ: 90°
• Cell volume: 6761 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1109
• Residual factor for significantly intense reflections: 0.0675
• Weighted residual factors for significantly intense reflections: 0.1219
• Weighted residual factors for all reflections included in the refinement: 0.1418
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No