Information card for entry 7003908

Structure parameters

• Formula: C34 H43 Cl Ge N2 O5 W
• Calculated formula: C34 H43 Cl Ge N2 O5 W
• Title of publication: Synthesis, characterisation and reactivity of germanium(ii) amidinate and guanidinate complexes
• Authors of publication: Jones, Cameron; Rose, Richard P.; Stasch, Andreas
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 21
• Pages of publication: 2871 - 2878
• a: 10.592 ± 0.002 Å
• b: 16.684 ± 0.003 Å
• c: 21.013 ± 0.004 Å
• α: 90°
• β: 101.67 ± 0.03°
• γ: 90°
• Cell volume: 3636.6 ± 1.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0424
• Residual factor for significantly intense reflections: 0.0335
• Weighted residual factors for significantly intense reflections: 0.0748
• Weighted residual factors for all reflections included in the refinement: 0.0788
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No