Information card for entry 7004855

Structure parameters

• Common name: trans-Dichlorobis(1,3- bis(dimethylphosphino)propane)cobalt(iii) Perchlorate
• Chemical name: trans-Dichlorobis(1,3-bis(dimethylphosphino)propane)cobalt(III) Perchlorate
• Formula: C14 H36 Cl3 Co O4 P4
• Calculated formula: C14 H36 Cl3 Co O4 P4
• Title of publication: Preparation and characterization of mixed-ligand cobalt(III) complexes containing (3-aminopropyl)dimethylphosphine (pdmp). Conformation of the six-membered pdmp chelate ring.
• Authors of publication: Suzuki, Takayoshi; Fujiiwara, Katsuhiro; Takagi, Hideo D.; Kashiwabara, Kazuo
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 3
• Pages of publication: 308 - 319
• a: 11.4228 ± 0.0015 Å
• b: 11.4228 ± 0.0015 Å
• c: 18.262 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2382.8 ± 0.6 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 133
• Hermann-Mauguin space group symbol: P 42/n b c :2
• Hall space group symbol: -P 4ac 2b
• Residual factor for all reflections: 0.0656
• Residual factor for significantly intense reflections: 0.0427
• Weighted residual factors for significantly intense reflections: 0.122
• Weighted residual factors for all reflections included in the refinement: 0.1354
• Goodness-of-fit parameter for all reflections included in the refinement: 1.095
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No