Information card for entry 7006086

Structure parameters

• Formula: C16 H56 F17 N8 O7 V4
• Calculated formula: C16 H56 F17 N8 O7 V4
• Title of publication: The role of temperature in the solvothermal synthesis of hybrid vanadium oxyfluorides
• Authors of publication: Aldous, David W.; Stephens, Nicholas F.; Lightfoot, Philip
• Journal of publication: Dalton Transactions
• Year of publication: 2007
• Journal issue: 37
• Pages of publication: 4207
• a: 12.873 ± 0.0014 Å
• b: 12.7838 ± 0.0015 Å
• c: 21.771 ± 0.002 Å
• α: 91.217 ± 0.004°
• β: 90.464 ± 0.004°
• γ: 92.179 ± 0.004°
• Cell volume: 3579.2 ± 0.7 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0322
• Residual factor for significantly intense reflections: 0.0298
• Weighted residual factors for significantly intense reflections: 0.0764
• Weighted residual factors for all reflections included in the refinement: 0.0787
• Goodness-of-fit parameter for all reflections included in the refinement: 0.984
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No