Information card for entry 7006087

Structure parameters

• Formula: C16 H52 F20 N8 O5 V5
• Calculated formula: C16 H48 F20 N8 O5 V5
• Title of publication: The role of temperature in the solvothermal synthesis of hybrid vanadium oxyfluorides
• Authors of publication: Aldous, David W.; Stephens, Nicholas F.; Lightfoot, Philip
• Journal of publication: Dalton Transactions
• Year of publication: 2007
• Journal issue: 37
• Pages of publication: 4207
• a: 11.7781 ± 0.0017 Å
• b: 12.524 ± 0.0018 Å
• c: 13.3317 ± 0.0019 Å
• α: 86.675 ± 0.002°
• β: 84.838 ± 0.002°
• γ: 67.417 ± 0.002°
• Cell volume: 1807.8 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0776
• Residual factor for significantly intense reflections: 0.0651
• Weighted residual factors for significantly intense reflections: 0.1668
• Weighted residual factors for all reflections included in the refinement: 0.1755
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.846 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No