Information card for entry 7006232

Structure parameters

• Formula: C252 H363 Ga16 N32 O81.5
• Calculated formula: C252 H118 Ga16 N32 O81.5
• Title of publication: Two octanuclear gallium metallamacrocycles of topologically different connectivities.
• Authors of publication: Park, Mira; John, Rohith P.; Moon, Dohyun; Lee, Kyungjin; Kim, Ghyung Hwa; Lah, Myoung Soo
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 46
• Pages of publication: 5412 - 5418
• a: 49.314 ± 0.01 Å
• b: 19.934 ± 0.004 Å
• c: 36.554 ± 0.007 Å
• α: 90°
• β: 127.1 ± 0.03°
• γ: 90°
• Cell volume: 28660 ± 15 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 5
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0732
• Residual factor for significantly intense reflections: 0.055
• Weighted residual factors for significantly intense reflections: 0.1484
• Weighted residual factors for all reflections included in the refinement: 0.1607
• Goodness-of-fit parameter for all reflections included in the refinement: 0.986
• Diffraction radiation wavelength: 0.7 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No