Information card for entry 7006233

Structure parameters

• Formula: C109.5 H146 Ga8 N31 O45
• Calculated formula: C109.6 H120 Ga8 N31 O45
• Title of publication: Two octanuclear gallium metallamacrocycles of topologically different connectivities.
• Authors of publication: Park, Mira; John, Rohith P.; Moon, Dohyun; Lee, Kyungjin; Kim, Ghyung Hwa; Lah, Myoung Soo
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 46
• Pages of publication: 5412 - 5418
• a: 24.973 ± 0.005 Å
• b: 26.951 ± 0.005 Å
• c: 27.543 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 18538 ± 6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0653
• Residual factor for significantly intense reflections: 0.0437
• Weighted residual factors for significantly intense reflections: 0.1036
• Weighted residual factors for all reflections included in the refinement: 0.1098
• Goodness-of-fit parameter for all reflections included in the refinement: 0.936
• Diffraction radiation wavelength: 0.7 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No