Information card for entry 7006252

Structure parameters

• Formula: C132 H160 Br2 Cl4 N10 O26 P8 Rh2 W2
• Calculated formula: C132 H136 Br2 Cl4 N10 O26 P8 Rh2 W2
• Title of publication: The oxadiazolyldiazenido(1-) ligand: a remarkably versatile platform for the synthesis of heteropolynuclear transition metal complexes.
• Authors of publication: Colquhoun, Howard M.; Chan, Yun Fu; Cardin, Christine J.; Drew, Michael G. B.; Gan, Yu; Abd El Kader, Kareem; White, Terence M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 35
• Pages of publication: 3864 - 3867
• a: 14.2326 ± 0.0015 Å
• b: 26.598 ± 0.003 Å
• c: 21.292 ± 0.002 Å
• α: 90°
• β: 108.357 ± 0.01°
• γ: 90°
• Cell volume: 7650.1 ± 1.5 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1625
• Residual factor for significantly intense reflections: 0.0794
• Weighted residual factors for significantly intense reflections: 0.1939
• Weighted residual factors for all reflections included in the refinement: 0.233
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No