Information card for entry 7006253

Structure parameters

• Formula: C75 H76 Br Fe N5 O4 P4 Pd W
• Calculated formula: C75 H75 Br Fe N5 O4 P4 Pd W
• Title of publication: The oxadiazolyldiazenido(1-) ligand: a remarkably versatile platform for the synthesis of heteropolynuclear transition metal complexes.
• Authors of publication: Colquhoun, Howard M.; Chan, Yun Fu; Cardin, Christine J.; Drew, Michael G. B.; Gan, Yu; Abd El Kader, Kareem; White, Terence M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 35
• Pages of publication: 3864 - 3867
• a: 12.1773 ± 0.0007 Å
• b: 14.9382 ± 0.001 Å
• c: 20.6774 ± 0.0012 Å
• α: 72.028 ± 0.006°
• β: 87.447 ± 0.005°
• γ: 74.688 ± 0.005°
• Cell volume: 3448 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0814
• Residual factor for significantly intense reflections: 0.0494
• Weighted residual factors for significantly intense reflections: 0.1164
• Weighted residual factors for all reflections included in the refinement: 0.1239
• Goodness-of-fit parameter for all reflections included in the refinement: 0.958
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No