Crystallography Open Database

Information card for entry 7006258

Preview

Coordinates	7006258.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H16 Br2 Ge6 Mn6 O32
Calculated formula	C38 H16 Br2 Ge6 Mn6 O32
Title of publication	Ge4Br4[Mn(CO)5]4 and Ge6Br2[Mn(CO)5]6: first germanium cluster compounds containing Mn(CO)5 ligands.
Authors of publication	Schenk, Christian; Schnepf, Andreas
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2007
Journal issue	46
Pages of publication	5400 - 5404
a	11.8044 ± 0.0009 Å
b	12.0886 ± 0.001 Å
c	20.6794 ± 0.0017 Å
α	92.677 ± 0.007°
β	98.768 ± 0.006°
γ	97.127 ± 0.006°
Cell volume	2887.4 ± 0.4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	155 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0856
Residual factor for significantly intense reflections	0.0563
Weighted residual factors for significantly intense reflections	0.1417
Weighted residual factors for all reflections included in the refinement	0.1567
Goodness-of-fit parameter for all reflections included in the refinement	0.985
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7006258.html