Information card for entry 7006259

Structure parameters

• Formula: C28 H16 Br4 Ge4 Mn4 O22
• Calculated formula: C28 H16 Br4 Ge4 Mn4 O22
• Title of publication: Ge4Br4[Mn(CO)5]4 and Ge6Br2[Mn(CO)5]6: first germanium cluster compounds containing Mn(CO)5 ligands.
• Authors of publication: Schenk, Christian; Schnepf, Andreas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 46
• Pages of publication: 5400 - 5404
• a: 11.34 ± 0.002 Å
• b: 13.759 ± 0.003 Å
• c: 15.402 ± 0.003 Å
• α: 82.29 ± 0.03°
• β: 78.9 ± 0.03°
• γ: 78.83 ± 0.03°
• Cell volume: 2301.8 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0887
• Residual factor for significantly intense reflections: 0.052
• Weighted residual factors for significantly intense reflections: 0.1098
• Weighted residual factors for all reflections included in the refinement: 0.1229
• Goodness-of-fit parameter for all reflections included in the refinement: 0.998
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No