Information card for entry 7007531

Structure parameters

• Formula: H31 K9 Ni O85.5 Si2 W20
• Calculated formula: K9 Ni O85.5 Si2 W20
• Title of publication: Transition metal containing decatungstosilicate dimer [M(H(2)O)(2)(gamma-SiW(10)O(35))(2)](10-) (M = Mn(2+), Co(2+), Ni(2+)).
• Authors of publication: Bassil, Bassem S.; Dickman, Michael H.; Reicke, Markus; Kortz, Ulrich; Keita, Bineta; Nadjo, Louis
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 35
• Pages of publication: 4253 - 4259
• a: 12.5354 ± 0.0006 Å
• b: 18.9293 ± 0.0009 Å
• c: 21.5454 ± 0.001 Å
• α: 107.78 ± 0.002°
• β: 101.753 ± 0.002°
• γ: 97.315 ± 0.002°
• Cell volume: 4666.6 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1187
• Residual factor for significantly intense reflections: 0.0675
• Weighted residual factors for significantly intense reflections: 0.1854
• Weighted residual factors for all reflections included in the refinement: 0.2179
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No