Information card for entry 7007532

Structure parameters

• Formula: Co H38 K10 O81.5 Si2 W20
• Calculated formula: Co K10 O81.5 Si2 W20
• Title of publication: Transition metal containing decatungstosilicate dimer [M(H(2)O)(2)(gamma-SiW(10)O(35))(2)](10-) (M = Mn(2+), Co(2+), Ni(2+)).
• Authors of publication: Bassil, Bassem S.; Dickman, Michael H.; Reicke, Markus; Kortz, Ulrich; Keita, Bineta; Nadjo, Louis
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 35
• Pages of publication: 4253 - 4259
• a: 18.907 ± 0.003 Å
• b: 22.688 ± 0.003 Å
• c: 24.795 ± 0.004 Å
• α: 63.048 ± 0.003°
• β: 79.31 ± 0.003°
• γ: 71.193 ± 0.003°
• Cell volume: 8965 ± 2 ų
• Cell temperature: 297 ± 2 K
• Ambient diffraction temperature: 297 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1561
• Residual factor for significantly intense reflections: 0.0793
• Weighted residual factors for significantly intense reflections: 0.2216
• Weighted residual factors for all reflections included in the refinement: 0.2752
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No