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Information card for entry 7007881
Preview
Coordinates | 7007881.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | bis((mu!2$-1-4-7-10-tetra-azacyclododecane-1,4,7,10-tetrayl- methyl-(trimethylene-tris(phenylphosphinato)))-gadolinium(iii)) decahydrate |
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Chemical name | bis((μ~2~-1-4-7-10-tetra-azacyclododecane-1,4,7,10-tetrayl-methyl- (trimethylene-tris(phenylphosphinato)))-gadolinium(III)) decahydrate |
Formula | C64 H108 Gd2 N8 O22 P6 |
Calculated formula | C64 H108 Gd2 N8 O22 P6 |
Title of publication | Synthesis and characterisation of dimeric eight-coordinate lanthanide(III) complexes of a macrocyclic tribenzylphosphinate ligand. |
Authors of publication | Senanayake, Kanthi; Thompson, Amber L.; Howard, Judith A. K.; Botta, Mauro; Parker, David |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2006 |
Journal issue | 45 |
Pages of publication | 5423 - 5428 |
a | 16.6618 ± 0.0007 Å |
b | 15.133 ± 0.0006 Å |
c | 30.2751 ± 0.0013 Å |
α | 90° |
β | 97.029 ± 0.001° |
γ | 90° |
Cell volume | 7576.3 ± 0.5 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 6 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0498 |
Residual factor for significantly intense reflections | 0.0271 |
Weighted residual factors for significantly intense reflections | 0.0418 |
Weighted residual factors for all reflections included in the refinement | 0.0473 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.908 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7007881.html
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Users of the data should acknowledge the original authors of the
structural data.