Information card for entry 7007882

Structure parameters

• Common name: bis((mu!2$-1-4-7-10-tetra-azacyclododecane-1,4,7,10-tetrayl- methyl-(trimethylene-tris(phenylphosphinato)))-europium(iii)) decahydrate
• Chemical name: bis((μ~2~-1-4-7-10-tetra-azacyclododecane-1,4,7,10-tetrayl-methyl- (trimethylene-tris(phenylphosphinato)))-europium(III)) decahydrate
• Formula: C64 H108 Eu2 N8 O22 P6
• Calculated formula: C64 H108 Eu2 N8 O22 P6
• Title of publication: Synthesis and characterisation of dimeric eight-coordinate lanthanide(III) complexes of a macrocyclic tribenzylphosphinate ligand.
• Authors of publication: Senanayake, Kanthi; Thompson, Amber L.; Howard, Judith A. K.; Botta, Mauro; Parker, David
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 45
• Pages of publication: 5423 - 5428
• a: 16.6586 ± 0.0008 Å
• b: 15.1326 ± 0.0007 Å
• c: 30.2862 ± 0.0015 Å
• α: 90°
• β: 97.014 ± 0.001°
• γ: 90°
• Cell volume: 7577.6 ± 0.6 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0833
• Residual factor for significantly intense reflections: 0.0689
• Weighted residual factors for significantly intense reflections: 0.1062
• Weighted residual factors for all reflections included in the refinement: 0.1092
• Goodness-of-fit parameter for all reflections included in the refinement: 1.42
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No