Information card for entry 7007883

Structure parameters

• Common name: bis((mu!2$-1-4-7-10-tetra-azacyclododecane-1,4,7,10-tetrayl- methyl-(trimethylene-tris(phenylphosphinato)))-europium(iii)) tridecahydrate
• Chemical name: bis((μ~2~-1-4-7-10-tetra-azacyclododecane-1,4,7,10-tetrayl-methyl- (trimethylene-tris(phenylphosphinato)))-europium(III)) tridecahydrate
• Formula: C64 H114 Eu2 N8 O25 P6
• Calculated formula: C64 H88 Eu2 N8 O25 P6
• Title of publication: Synthesis and characterisation of dimeric eight-coordinate lanthanide(III) complexes of a macrocyclic tribenzylphosphinate ligand.
• Authors of publication: Senanayake, Kanthi; Thompson, Amber L.; Howard, Judith A. K.; Botta, Mauro; Parker, David
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 45
• Pages of publication: 5423 - 5428
• a: 11.2286 ± 0.0012 Å
• b: 11.2774 ± 0.0012 Å
• c: 16.8782 ± 0.0017 Å
• α: 98.094 ± 0.002°
• β: 107.307 ± 0.002°
• γ: 97.237 ± 0.002°
• Cell volume: 1988.1 ± 0.4 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1149
• Residual factor for significantly intense reflections: 0.0613
• Weighted residual factors for significantly intense reflections: 0.1009
• Weighted residual factors for all reflections included in the refinement: 0.1168
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No