Information card for entry 7008453

Structure parameters

• Formula: C42 H42 Cl4 N4 P2 Pt
• Calculated formula: C42 H42 Cl4 N4 P2 Pt
• Title of publication: The first examples of metal-mediated addition of a phosphorus imine to nitriles; the preparation and X-ray crystal structures of [PtCl4{NH=C(Et)N=PPh3}2] and [PtCl2(EtCN){NH=C(Et)N[double bond, length as m-dash]PPh3}].
• Authors of publication: Bokach, Nadezhda A.; Kukushkin, Vadim Yu; Kelly, Paul F.; Haukka, Matti; Pombeiro, Armando J. L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 8
• Pages of publication: 1354 - 1356
• a: 10.121 ± 0.0002 Å
• b: 13.7987 ± 0.0004 Å
• c: 15.6217 ± 0.0004 Å
• α: 73.89 ± 0.001°
• β: 86.897 ± 0.002°
• γ: 89.625 ± 0.002°
• Cell volume: 2092.85 ± 0.09 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0468
• Residual factor for significantly intense reflections: 0.0301
• Weighted residual factors for significantly intense reflections: 0.0695
• Weighted residual factors for all reflections included in the refinement: 0.0761
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No