Information card for entry 7008718

Structure parameters

• Formula: C60 H100 Cr2 N4 O6 Si4
• Calculated formula: C52 H84 Cr2 N4 O4 Si4
• Title of publication: Synthesis of mixed-donor amido/amino/siloxo ligands from symmetrical diamidosilylether ligands via a retro-Brook rearrangement and their chromium(ii) complexes
• Authors of publication: Haftbaradaran, Farzad; Mund, Garry; Batchelor, Raymond J.; Britten, James F.; Leznoff, Daniel B.
• Journal of publication: Dalton Transactions
• Year of publication: 2005
• Journal issue: 14
• Pages of publication: 2343
• a: 11.146 ± 0.003 Å
• b: 27.506 ± 0.007 Å
• c: 22.192 ± 0.005 Å
• α: 90°
• β: 99.63 ± 0.004°
• γ: 90°
• Cell volume: 6708 ± 3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0729
• Residual factor for significantly intense reflections: 0.0451
• Weighted residual factors for significantly intense reflections: 0.1226
• Weighted residual factors for all reflections included in the refinement: 0.1339
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No