Information card for entry 7008771

Structure parameters

• Common name: [{C6H4(NCH2tBu)2}Si(Cl)Si(CH2Cl){(NCH2tBu)2C6H4}
• Formula: C33 H54 Cl2 N4 Si2
• Calculated formula: C33 H54 Cl2 N4 Si2
• Title of publication: Reactions of a stable silylene with halocarbons
• Authors of publication: Delawar, Mahmood; Gehrhus, Barbara; Hitchcock, Peter B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 17
• Pages of publication: 2945 - 2953
• a: 10.2646 ± 0.0005 Å
• b: 18.5123 ± 0.001 Å
• c: 10.618 ± 0.0005 Å
• α: 99.309 ± 0.003°
• β: 70.322 ± 0.003°
• γ: 82.774 ± 0.003°
• Cell volume: 1839.18 ± 0.17 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0958
• Residual factor for significantly intense reflections: 0.0841
• Weighted residual factors for significantly intense reflections: 0.1954
• Weighted residual factors for all reflections included in the refinement: 0.2009
• Goodness-of-fit parameter for all reflections included in the refinement: 1.239
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No