Information card for entry 7008881

Structure parameters

• Formula: C53.5 H85.5 O12 Si8 Sn
• Calculated formula: C53.25 H84.25 O12 Si8 Sn
• Title of publication: Silsesquioxane-bonded zirconocene complexes; soluble models for silica-tethered olefin polymerization catalysts
• Authors of publication: Severn, John R.; Duchateau, Robbert; van Santen, Rutger A.; Ellis, Dianne D.; Spek, Anthony L.; Yap, Glenn P. A.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 11
• Pages of publication: 2293
• a: 10.932 ± 0.0003 Å
• b: 17.973 ± 0.0004 Å
• c: 32.016 ± 0.0007 Å
• α: 90°
• β: 94.0678 ± 0.0008°
• γ: 90°
• Cell volume: 6274.7 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 c 1
• Hall space group symbol: P -2yc
• Residual factor for all reflections: 0.0875
• Residual factor for significantly intense reflections: 0.0708
• Weighted residual factors for significantly intense reflections: 0.1643
• Weighted residual factors for all reflections included in the refinement: 0.1738
• Goodness-of-fit parameter for all reflections included in the refinement: 1.084
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No