Information card for entry 7008882

Structure parameters

• Formula: C55 H86 O12 Si8
• Calculated formula: C55 H86 O12 Si8
• Title of publication: Silsesquioxane-bonded zirconocene complexes; soluble models for silica-tethered olefin polymerization catalysts
• Authors of publication: Severn, John R.; Duchateau, Robbert; van Santen, Rutger A.; Ellis, Dianne D.; Spek, Anthony L.; Yap, Glenn P. A.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 11
• Pages of publication: 2293
• a: 10.489 ± 0.001 Å
• b: 30.222 ± 0.003 Å
• c: 19.52 ± 0.002 Å
• α: 90°
• β: 91.441 ± 0.002°
• γ: 90°
• Cell volume: 6185.9 ± 1.1 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0886
• Residual factor for significantly intense reflections: 0.0479
• Weighted residual factors for significantly intense reflections: 0.108
• Weighted residual factors for all reflections included in the refinement: 0.1191
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No