Information card for entry 7008980

Structure parameters

• Formula: C36 H52 P2 Pd2 Si2
• Calculated formula: C36 H52 P2 Pd2 Si2
• SMILES: [P](CC)(CC)([Pd]123[H][Si]2(c2ccccc2)(c2ccccc2)[Pd]21([P](CC)(CC)CC)[H][Si]32(c1ccccc1)c1ccccc1)CC
• Title of publication: Dipalladium complexes with bridging diorganosilyl ligands. Synthesis, structure, and properties of [LPd(μ-SiH(R)Ph)]2 (R = Ph or Me; L = PMe3, PEt3 or PMePh2)
• Authors of publication: Kim, Yong-Joo; Lee, Sang-Chul; Park, Jong-Il; Osakada, Kohtaro; Choi, Jun-Chul; Yamamoto, Takakazu
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 3
• Pages of publication: 417
• a: 10.242 ± 0.009 Å
• b: 11.447 ± 0.006 Å
• c: 9.725 ± 0.008 Å
• α: 112.13 ± 0.05°
• β: 115.65 ± 0.06°
• γ: 78.56 ± 0.06°
• Cell volume: 951.2 ± 1.4 ų
• Cell temperature: 296.2 K
• Ambient diffraction temperature: 296.2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.038
• Weighted residual factors for all reflections included in the refinement: 0.045
• Goodness-of-fit parameter for all reflections included in the refinement: 2.57
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No