Information card for entry 7008981

Structure parameters

• Formula: C20 H36 P2 Pd2 Si2
• Calculated formula: C20 H36 P2 Pd2 Si2
• SMILES: C[P](C)(C)[Pd]123[Si]4(C)(c5ccccc5)[H][Pd]24([P](C)(C)C)[Si]3(C)(c2ccccc2)[H]1
• Title of publication: Dipalladium complexes with bridging diorganosilyl ligands. Synthesis, structure, and properties of [LPd(μ-SiH(R)Ph)]2 (R = Ph or Me; L = PMe3, PEt3 or PMePh2)
• Authors of publication: Kim, Yong-Joo; Lee, Sang-Chul; Park, Jong-Il; Osakada, Kohtaro; Choi, Jun-Chul; Yamamoto, Takakazu
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 3
• Pages of publication: 417
• a: 8.419 ± 0.004 Å
• b: 16.222 ± 0.004 Å
• c: 10.24 ± 0.004 Å
• α: 90°
• β: 108.58 ± 0.03°
• γ: 90°
• Cell volume: 1325.6 ± 0.9 ų
• Cell temperature: 296.2 K
• Ambient diffraction temperature: 296.2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.033
• Weighted residual factors for all reflections included in the refinement: 0.036
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No