Information card for entry 7009097

Structure parameters

• Formula: C28 H59 As Li N4 O P3
• Calculated formula: C28 H59 As Li N4 O P3
• SMILES: [As]1(P(P(P1C(C)(C)C)C(C)(C)C)C(C)(C)C)[Li]([N]12CCN(CC1)CC2)([N]12CCN(CC2)CC1)[O]1CCCC1
• Title of publication: A synthetic and structural study of the formation of cyclic [(RP)nE]− anions and Zintl compounds using E(NMe2)3 (E = As, Sb)
• Authors of publication: Bashall, Alan; Beswick, Michael A.; Choi, Nick; Hopkins, Alexander D.; Kidd, Sara J.; Lawson, Yvonne G.; Mosquera, Marta E. G.; McPartlin, Mary; Raithby, Paul R.; Wheatley, Andrew A. E. H.; Wood, Jody A.; Wright, Dominic S.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 4
• Pages of publication: 479
• a: 11.651 ± 0.002 Å
• b: 12.638 ± 0.003 Å
• c: 13.991 ± 0.003 Å
• α: 71.11 ± 0.03°
• β: 73.79 ± 0.03°
• γ: 64.61 ± 0.03°
• Cell volume: 1737 ± 0.8 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0559
• Residual factor for significantly intense reflections: 0.0362
• Weighted residual factors for all reflections: 0.1173
• Weighted residual factors for significantly intense reflections: 0.0901
• Goodness-of-fit parameter for all reflections: 1.082
• Goodness-of-fit parameter for significantly intense reflections: 0.937
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No