Information card for entry 7009103

Structure parameters

• Formula: C67.65 H57.53 Ag B Cl0.48 F4 N1.68 P4 S8
• Calculated formula: C67.636 H57.516 Ag B Cl0.494 F4 N1.674 P4 S8
• Title of publication: Homoleptic complexes of Ag(I), Cu(I), Pd(II) and Pt(II) with tetrathiafulvalene-functionalized phosphine ligands †
• Authors of publication: Smucker, Bradley W.; Dunbar, Kim R.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 8
• Pages of publication: 1309
• a: 25.569 ± 0.005 Å
• b: 21.376 ± 0.004 Å
• c: 27.209 ± 0.005 Å
• α: 90°
• β: 112.75 ± 0.03°
• γ: 90°
• Cell volume: 13714 ± 5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0701
• Residual factor for significantly intense reflections: 0.0409
• Weighted residual factors for significantly intense reflections: 0.1171
• Weighted residual factors for all reflections included in the refinement: 0.1345
• Goodness-of-fit parameter for all reflections included in the refinement: 0.9
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No