Information card for entry 7009271

Structure parameters

• Formula: C33 H54 F2.5 Fe3 Ga2 O10 Si6
• Calculated formula: C33 H54 F2.49 Fe3 Ga2 O10 Si6
• Title of publication: Replacement of CO ligands by the isolobal gallium(I) compound GaR [R = C(SiMe3)3], formation of the transition metal gallium compounds Mn2(CO)8(μ-GaR)2 and Fe3(CO)9(μ-CO)(μ-GaR)2
• Authors of publication: Uhl, Werner; Benter, Maike; Prött, Malte
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 5
• Pages of publication: 643
• a: 9.3853 ± 0.0009 Å
• b: 14.757 ± 0.002 Å
• c: 19.118 ± 0.002 Å
• α: 75.71 ± 0.02°
• β: 80.74 ± 0.01°
• γ: 74.49 ± 0.01°
• Cell volume: 2459.6 ± 0.5 ų
• Cell temperature: 213 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0434
• Residual factor for significantly intense reflections: 0.0327
• Weighted residual factors for significantly intense reflections: 0.0849
• Weighted residual factors for all reflections included in the refinement: 0.0944
• Goodness-of-fit parameter for all reflections included in the refinement: 0.674
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No