Information card for entry 7009273

Structure parameters

• Formula: C32 H27 B Cu F4 N6 O2
• Calculated formula: C32 H27 B Cu F4 N6 O2
• Title of publication: Effects of metal co-ordination geometry on self-assembly: a dinuclear double helicate complex and a tetranuclear cage complex of a new bis-bidentate bridging ligand
• Authors of publication: Paul, Rowena L.; Couchman, Samantha M.; Jeffery, John C.; McCleverty, Jon A.; Reeves, Zoe R.; Ward, Michael D.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 6
• Pages of publication: 845
• a: 14.702 ± 0.003 Å
• b: 20.284 ± 0.004 Å
• c: 20.669 ± 0.006 Å
• α: 90°
• β: 94.561 ± 0.011°
• γ: 90°
• Cell volume: 6144 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1452
• Residual factor for significantly intense reflections: 0.0654
• Weighted residual factors for all reflections: 0.1773
• Weighted residual factors for significantly intense reflections: 0.1442
• Goodness-of-fit parameter for all reflections: 0.954
• Goodness-of-fit parameter for significantly intense reflections: 1.112
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No