Information card for entry 7009274

Structure parameters

• Formula: C192 H162 B8 Co4 F32 N42
• Calculated formula: C197 H144 B7.98 Co4 F31.92 N38.5
• Title of publication: Effects of metal co-ordination geometry on self-assembly: a dinuclear double helicate complex and a tetranuclear cage complex of a new bis-bidentate bridging ligand
• Authors of publication: Paul, Rowena L.; Couchman, Samantha M.; Jeffery, John C.; McCleverty, Jon A.; Reeves, Zoe R.; Ward, Michael D.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 6
• Pages of publication: 845
• a: 19.221 ± 0.008 Å
• b: 37.421 ± 0.018 Å
• c: 31.929 ± 0.009 Å
• α: 90°
• β: 90.71 ± 0.02°
• γ: 90°
• Cell volume: 22964 ± 16 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.2633
• Residual factor for significantly intense reflections: 0.1576
• Weighted residual factors for significantly intense reflections: 0.4077
• Weighted residual factors for all reflections included in the refinement: 0.4853
• Goodness-of-fit parameter for all reflections included in the refinement: 1.589
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No