Information card for entry 7009277

Structure parameters

• Formula: C64 H76 Mo2 N4 O6 Si4
• Calculated formula: C64 H76 Mo2 N4 O6 Si4
• Title of publication: High oxidation state imido metallasiloxanes: synthesis and structural characterisation of novel bis-imido chromium(VI) and molybdenum(VI) compounds †
• Authors of publication: King, Lawrence; Motevalli, Majid; Sullivan, Alice C.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 8
• Pages of publication: 1357
• a: 12.395 ± 0.002 Å
• b: 15.831 ± 0.003 Å
• c: 17.246 ± 0.003 Å
• α: 90°
• β: 100.07 ± 0.03°
• γ: 90°
• Cell volume: 3332 ± 1.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2106
• Residual factor for significantly intense reflections: 0.0867
• Weighted residual factors for significantly intense reflections: 0.2059
• Weighted residual factors for all reflections included in the refinement: 0.2454
• Goodness-of-fit parameter for all reflections included in the refinement: 0.923
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No