Information card for entry 7009278

Structure parameters

• Formula: C37.5 H47.5 Cl2 Mo N4
• Calculated formula: C37.5 H47.5 Cl2 Mo N4
• Title of publication: High oxidation state imido metallasiloxanes: synthesis and structural characterisation of novel bis-imido chromium(VI) and molybdenum(VI) compounds †
• Authors of publication: King, Lawrence; Motevalli, Majid; Sullivan, Alice C.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 8
• Pages of publication: 1357
• a: 9.689 ± 0.006 Å
• b: 37.658 ± 0.008 Å
• c: 10.246 ± 0.004 Å
• α: 90°
• β: 95.62 ± 0.05°
• γ: 90°
• Cell volume: 3720 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1639
• Residual factor for significantly intense reflections: 0.1067
• Weighted residual factors for all reflections: 0.3358
• Weighted residual factors for significantly intense reflections: 0.2893
• Goodness-of-fit parameter for all reflections: 0.914
• Goodness-of-fit parameter for significantly intense reflections: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No