Information card for entry 7009452

Structure parameters

• Formula: C17 H35 Cl Co Ge O9 P3
• Calculated formula: C17 H35 Cl Co Ge O9 P3
• Title of publication: Oxidation of germanium(II) azides with HN3: a convenient route to six-co-ordinate triazidogermanium(IV) compounds
• Authors of publication: Filippou, Alexander C.; Portius, Peter; Kociok-Köhn, Gabriele; Albrecht, Volker
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 11
• Pages of publication: 1759
• a: 12.219 ± 0.003 Å
• b: 14.26 ± 0.005 Å
• c: 15.304 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2666.6 ± 1.3 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0322
• Residual factor for significantly intense reflections: 0.0248
• Weighted residual factors for significantly intense reflections: 0.0442
• Weighted residual factors for all reflections included in the refinement: 0.0455
• Goodness-of-fit parameter for all reflections included in the refinement: 0.944
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No