Information card for entry 7009453

Structure parameters

• Formula: C15 H22 B Ge N15
• Calculated formula: C15 H22 B Ge N15
• SMILES: [Ge]12([n]3c(C)cc(C)n3[BH](n3[n]1c(C)cc3C)n1[n]2c(C)cc1C)(N=N#N)(N=N#N)N=N#N
• Title of publication: Oxidation of germanium(II) azides with HN3: a convenient route to six-co-ordinate triazidogermanium(IV) compounds
• Authors of publication: Filippou, Alexander C.; Portius, Peter; Kociok-Köhn, Gabriele; Albrecht, Volker
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 11
• Pages of publication: 1759
• a: 11.378 ± 0.007 Å
• b: 10.918 ± 0.013 Å
• c: 17.719 ± 0.009 Å
• α: 90°
• β: 101.04 ± 0.04°
• γ: 90°
• Cell volume: 2160 ± 3 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0441
• Residual factor for significantly intense reflections: 0.0413
• Weighted residual factors for significantly intense reflections: 0.1135
• Weighted residual factors for all reflections included in the refinement: 0.1166
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No