Crystallography Open Database

Information card for entry 7009455

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Coordinates	7009455.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C17 H35 Co Ge N9 O9 P3
Calculated formula	C17 H35 Co Ge N9 O9 P3
Title of publication	Oxidation of germanium(II) azides with HN3: a convenient route to six-co-ordinate triazidogermanium(IV) compounds
Authors of publication	Filippou, Alexander C.; Portius, Peter; Kociok-Köhn, Gabriele; Albrecht, Volker
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	11
Pages of publication	1759
a	17.1284 ± 0.0014 Å
b	12.0633 ± 0.001 Å
c	14.6659 ± 0.0008 Å
α	90°
β	97.283 ± 0.008°
γ	90°
Cell volume	3005.9 ± 0.4 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	7
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0565
Residual factor for significantly intense reflections	0.0522
Weighted residual factors for significantly intense reflections	0.136
Weighted residual factors for all reflections included in the refinement	0.1411
Goodness-of-fit parameter for all reflections included in the refinement	1.069
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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