Information card for entry 7009454

Structure parameters

• Formula: C17 H35 Co Ge N3 O9 P3
• Calculated formula: C17 H35 Co Ge N3 O9 P3
• SMILES: [Co]123456([cH]7[cH]4[cH]3[cH]2[cH]17)[P](OCC)(OCC)[O][Ge](O[P]5(OCC)OCC)(O[P]6(OCC)OCC)N=N#N
• Title of publication: Oxidation of germanium(II) azides with HN3: a convenient route to six-co-ordinate triazidogermanium(IV) compounds
• Authors of publication: Filippou, Alexander C.; Portius, Peter; Kociok-Köhn, Gabriele; Albrecht, Volker
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 11
• Pages of publication: 1759
• a: 8.458 ± 0.0012 Å
• b: 17.226 ± 0.002 Å
• c: 18.673 ± 0.004 Å
• α: 90°
• β: 93.29 ± 0.02°
• γ: 90°
• Cell volume: 2716.1 ± 0.8 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0897
• Residual factor for significantly intense reflections: 0.0425
• Weighted residual factors for significantly intense reflections: 0.0845
• Weighted residual factors for all reflections included in the refinement: 0.095
• Goodness-of-fit parameter for all reflections included in the refinement: 0.878
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No