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Information card for entry 7009475
Preview
Coordinates | 7009475.cif |
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Original paper (by DOI) | HTML |
Formula | C28 H56 N6 Na Sb3 |
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Calculated formula | C28 H56 N6 Na Sb3 |
SMILES | [Sb]12N(C3CCCCC3)[Sb]34N(C5CCCCC5)[Sb]5[N](C)(C)[Na]([N]35C3CCCCC3)([N]14C1CCCCC1)[N]2(C)C |
Title of publication | Reactions of the spiro monoanion [{(Me2N)Sb(μ-NCy)2}2Sb]− with alcohols and thiols (REH; E = O or S); syntheses of nido-[Sb3(μ-NCy)3(μ3-NCy)(ER)2] anions and the unique antimony(III) imido cubane [(2-NC5H4O)Sb(μ3-NCy)]4 (Cy= cyclohexyl) |
Authors of publication | Bashall, Alan; Beswick, Michael A.; Feeder, Neil; Hopkins, Alexander D.; Kidd, Sara J.; McPartlin, Mary; Raithby, Paul R.; Wright, Dominic S. |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 2000 |
Journal issue | 12 |
Pages of publication | 1841 |
a | 9.599 ± 0.002 Å |
b | 21.379 ± 0.004 Å |
c | 17.097 ± 0.003 Å |
α | 90° |
β | 99.82 ± 0.03° |
γ | 90° |
Cell volume | 3457.2 ± 1.2 Å3 |
Cell temperature | 180 ± 2 K |
Ambient diffraction temperature | 180 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1155 |
Residual factor for significantly intense reflections | 0.0787 |
Weighted residual factors for significantly intense reflections | 0.1986 |
Weighted residual factors for all reflections included in the refinement | 0.2259 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.002 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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Users of the data should acknowledge the original authors of the
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