Information card for entry 7009481

Structure parameters

• Formula: C10 H20 Cl2 F6 N4 O2 Rh Sb
• Calculated formula: C10 H20 Cl2 F6 N4 O2 Rh Sb
• Title of publication: Metal-mediated hydrolysis of the oxime CN bond to produce RhIII-bound O-iminoacylated MeC(NH)ONH2 species
• Authors of publication: Kukushkin, Vadim Yu.; Ilichev, Igor V.; Zhdanova, Maria A.; Wagner, Gabriele; Pombeiro, Armando J. L.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 10
• Pages of publication: 1567
• a: 12.293 ± 0.002 Å
• b: 10.021 ± 0.002 Å
• c: 8.811 ± 0.002 Å
• α: 90°
• β: 106.75 ± 0.03°
• γ: 90°
• Cell volume: 1039.4 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0439
• Residual factor for significantly intense reflections: 0.0439
• Weighted residual factors for significantly intense reflections: 0.1098
• Weighted residual factors for all reflections included in the refinement: 0.1098
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No