Information card for entry 7009482

Structure parameters

• Formula: C4 H12 Cl3 N4 O2 Rh
• Calculated formula: C4 H12 Cl3 N4 O2 Rh
• Title of publication: Metal-mediated hydrolysis of the oxime CN bond to produce RhIII-bound O-iminoacylated MeC(NH)ONH2 species
• Authors of publication: Kukushkin, Vadim Yu.; Ilichev, Igor V.; Zhdanova, Maria A.; Wagner, Gabriele; Pombeiro, Armando J. L.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 10
• Pages of publication: 1567
• a: 8.483 ± 0.002 Å
• b: 8.508 ± 0.002 Å
• c: 8.617 ± 0.002 Å
• α: 87.86 ± 0.03°
• β: 79.59 ± 0.03°
• γ: 80.42 ± 0.03°
• Cell volume: 603.1 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0276
• Residual factor for significantly intense reflections: 0.0276
• Weighted residual factors for significantly intense reflections: 0.078
• Weighted residual factors for all reflections included in the refinement: 0.078
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.56083 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No