Information card for entry 7009492

Structure parameters

• Formula: C24 H10 As Mo2 O14 P W2
• Calculated formula: C24 H10 As Mo2 O14 P W2
• Title of publication: The preparation of [M2Cp2(CO)4(μ-η2-PE)] (E = As or Sb), the first complexes with naked heterodiatomic Group 15 ligands, and of their adducts with W(CO)5
• Authors of publication: Davies, John E.; Mays, Martin J.; Raithby, Paul R.; Shields, Gregory P.; Tompkin, Peter K.; Woods, Anthony D.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 12
• Pages of publication: 1925
• a: 18.677 ± 0.005 Å
• b: 10.799 ± 0.005 Å
• c: 16.916 ± 0.005 Å
• α: 90°
• β: 110.22 ± 0.01°
• γ: 90°
• Cell volume: 3202 ± 2 ų
• Cell temperature: 290 ± 2 K
• Ambient diffraction temperature: 290 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0786
• Residual factor for significantly intense reflections: 0.0409
• Weighted residual factors for all reflections: 0.082
• Weighted residual factors for significantly intense reflections: 0.0702
• Goodness-of-fit parameter for all reflections: 0.999
• Goodness-of-fit parameter for significantly intense reflections: 1.054
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No