Information card for entry 7009493

Structure parameters

• Formula: C19 H10 Mo2 O9 P Sb W
• Calculated formula: C19 H10 Mo2 O9 P Sb W
• SMILES: [W]([P]12[Sb]([Mo]34562(C#[O])(C#[O])[cH]2[cH]3[cH]4[cH]5[cH]62)[Mo]23451(C#[O])(C#[O])[cH]1[cH]2[cH]3[cH]5[cH]41)(C#[O])(C#[O])(C#[O])(C#[O])C#[O]
• Title of publication: The preparation of [M2Cp2(CO)4(μ-η2-PE)] (E = As or Sb), the first complexes with naked heterodiatomic Group 15 ligands, and of their adducts with W(CO)5
• Authors of publication: Davies, John E.; Mays, Martin J.; Raithby, Paul R.; Shields, Gregory P.; Tompkin, Peter K.; Woods, Anthony D.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 12
• Pages of publication: 1925
• a: 15.974 ± 0.005 Å
• b: 16.236 ± 0.008 Å
• c: 10.623 ± 0.002 Å
• α: 97.85 ± 0.03°
• β: 96.34 ± 0.02°
• γ: 118.86 ± 0.02°
• Cell volume: 2340.4 ± 1.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0389
• Residual factor for significantly intense reflections: 0.035
• Weighted residual factors for all reflections: 0.0922
• Weighted residual factors for significantly intense reflections: 0.0896
• Goodness-of-fit parameter for all reflections: 1.092
• Goodness-of-fit parameter for significantly intense reflections: 1.111
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No