Information card for entry 7009510

Structure parameters

• Formula: C10 H30 N4 Ni O8
• Calculated formula: C10 H30 N4 Ni O8
• Title of publication: The crystal and molecular structures of the nickel(II) complexes of malonamide-derived unsubstituted 14- and 13-membered tetraazamacrocycles and NMR study of the complexes in aqueous solution
• Authors of publication: Yaroslaw D. Lampeka; Sergey P. Gavrish; Robert W. Hay; Tanja Eisenblätter; Philip Lightfoot
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2000
• Journal issue: 13
• Pages of publication: 2023 - 2029
• a: 7.247 ± 0.002 Å
• b: 24.982 ± 0.004 Å
• c: 9.436 ± 0.003 Å
• α: 90°
• β: 92.17 ± 0.03°
• γ: 90°
• Cell volume: 1707.1 ± 0.8 ų
• Cell temperature: 473.2 K
• Ambient diffraction temperature: 473.2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.0476
• Weighted residual factors for significantly intense reflections: 0.0541
• Goodness-of-fit parameter for significantly intense reflections: 3.464
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No