Information card for entry 7009511

Structure parameters

• Formula: C9 H26 N4 Ni O7
• Calculated formula: C9 H26 N4 Ni O7
• Title of publication: The crystal and molecular structures of the nickel(II) complexes of malonamide-derived unsubstituted 14- and 13-membered tetraazamacrocycles and NMR study of the complexes in aqueous solution
• Authors of publication: Yaroslaw D. Lampeka; Sergey P. Gavrish; Robert W. Hay; Tanja Eisenblätter; Philip Lightfoot
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2000
• Journal issue: 13
• Pages of publication: 2023 - 2029
• a: 9.892 ± 0.003 Å
• b: 11.279 ± 0.004 Å
• c: 7.352 ± 0.002 Å
• α: 94.48 ± 0.02°
• β: 102.43 ± 0.02°
• γ: 83.95 ± 0.03°
• Cell volume: 795.3 ± 0.4 ų
• Cell temperature: 293.2 K
• Ambient diffraction temperature: 293.2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0407
• Weighted residual factors for significantly intense reflections: 0.0398
• Goodness-of-fit parameter for significantly intense reflections: 2.909
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No